Table 1.  Crystal data and structure refinement for structure 56.

Identification code 	str0165
Chemical formula 	C19H28O2
Formula weight 	288.41
Temperature 	150(2) K
Radiation, wavelength 	MoKa, 0.71073 Å
Crystal system, space group 	orthorhombic, P212121
Unit cell parameters	a = 8.804(3) Å	a = 90°
	b = 10.274(3) Å	b = 90°
	c = 18.428(5) Å	g = 90°
Cell volume	1666.9(8) Å3
Z	4
Calculated density 	1.149 g/cm3
Absorption coefficient m	0.072 mm1
F(000)	632
Crystal colour and size	colourless, 0.50  0.04  0.02 mm3
Data collection method	Bruker SMART APEX diffractometer
	w rotation with narrow frames
q range for data collection	2.21 to 28.26°
Index ranges	h 11 to 11, k 13 to 13, l 23 to 23
Completeness to q = 26.00°	100.0 % 
Reflections collected	14443
Independent reflections	3899 (Rint = 0.0698)
Reflections with F2>2s	2927
Absorption correction	semi-empirical from equivalents
Min. and max. transmission	0.9648 and 0.9986
Structure solution	direct methods
Refinement method	Full-matrix least-squares on F2
Weighting parameters a, b	0.0660, 0.0000
Data / restraints / parameters	3899 / 0 / 194
Final R indices [F2>2s]	R1 = 0.0579, wR2 = 0.1220
R indices (all data)	R1 = 0.0817, wR2 = 0.1329
Goodness-of-fit on F2	0.987
Largest and mean shift/su	0.001 and 0.000
Largest diff. peak and hole	0.250 and 0.199 e Å3

Table 2.  Atomic coordinates and equivalent isotropic displacement parameters (Å2)
for str0165.  Ueq is defined as one third of the trace of the orthogonalized Uij tensor.

	     x	     y	     z	     Ueq

O(1)	0.15357(17)	0.16319(12)	1.03009(7)	0.0232(3)
O(2)	0.11113(18)	0.36569(12)	0.98012(7)	0.0255(4)
C(1)	0.1945(2)	0.29512(18)	1.03172(11)	0.0231(5)
C(2)	0.1615(2)	0.35216(19)	1.10605(11)	0.0240(5)
C(3)	0.1508(3)	0.4863(2)	1.11330(12)	0.0298(5)
C(4)	0.1287(3)	0.5414(2)	1.18130(12)	0.0359(6)
C(5)	0.1156(3)	0.4637(2)	1.24170(12)	0.0392(6)
C(6)	0.1262(3)	0.3299(2)	1.23427(12)	0.0384(6)
C(7)	0.1488(3)	0.2744(2)	1.16671(11)	0.0306(5)
C(8)	0.0462(3)	0.4146(2)	0.86171(12)	0.0386(6)
C(9)	0.1463(3)	0.32625(18)	0.90653(10)	0.0247(5)
C(10)	0.1223(2)	0.17812(18)	0.89768(10)	0.0211(4)
C(11)	0.1986(2)	0.10725(19)	0.96155(10)	0.0218(4)
C(12)	0.1700(2)	 0.03978(19)	0.96391(11)	0.0258(5)
C(13)	0.0040(3)	 0.0787(2)	0.98074(12)	0.0306(5)
C(14)	 0.0400(3)	 0.2141(2)	0.95222(14)	0.0440(7)
C(15)	 0.0298(3)	 0.0756(2)	1.06161(13)	0.0468(7)
C(16)	0.2340(3)	 0.0935(2)	0.89292(12)	0.0323(5)
C(17)	0.1638(3)	 0.0274(2)	0.82687(11)	0.0322(5)
C(18)	0.1857(3)	0.1206(2)	0.82657(11)	0.0287(5)
C(19)	0.1178(3)	0.1748(2)	0.75641(11)	0.0425(7)

Table 3.   Bond lengths [Å] and angles [°] for str0165.

O(1)–C(1) 	1.403(2)	O(1)–C(11) 	1.443(2)
O(2)–C(1) 	1.403(2)	O(2)–C(9) 	1.449(2)
C(1)–C(2) 	1.518(3)	C(2)–C(7) 	1.378(3)
C(2)–C(3) 	1.388(3)	C(3)–C(4) 	1.389(3)
C(4)–C(5) 	1.375(3)	C(5)–C(6) 	1.385(3)
C(6)–C(7) 	1.384(3)	C(8)–C(9) 	1.511(3)
C(9)–C(10) 	1.545(3)	C(10)–C(11) 	1.538(3)
C(10)–C(18) 	1.542(3)	C(11)–C(12) 	1.532(3)
C(12)–C(16) 	1.527(3)	C(12)–C(13) 	1.547(3)
C(13)–C(15) 	1.520(3)	C(13)–C(14) 	1.536(3)
C(16)–C(17) 	1.524(3)	C(17)–C(18) 	1.532(3)
C(18)–C(19) 	1.530(3)	

C(1)–O(1)–C(11)	109.45(15)	C(1)–O(2)–C(9)	112.21(15)
O(1)–C(1)–O(2)	110.50(16)	O(1)–C(1)–C(2)	110.07(17)
O(2)–C(1)–C(2)	108.17(16)	C(7)–C(2)–C(3)	119.5(2)
C(7)–C(2)–C(1)	121.58(18)	C(3)–C(2)–C(1)	118.89(19)
C(2)–C(3)–C(4)	120.1(2)	C(5)–C(4)–C(3)	120.4(2)
C(4)–C(5)–C(6)	119.4(2)	C(5)–C(6)–C(7)	120.5(2)
C(2)–C(7)–C(6)	120.2(2)	O(2)–C(9)–C(8)	102.66(17)
O(2)–C(9)–C(10)	110.19(15)	C(8)–C(9)–C(10)	117.04(18)
C(11)–C(10)–C(18)	108.10(16)	C(11)–C(10)–C(9)	109.02(16)
C(18)–C(10)–C(9)	114.72(16)	O(1)–C(11)–C(12)	108.82(16)
O(1)–C(11)–C(10)	111.16(15)	C(12)–C(11)–C(10)	114.63(16)
C(16)–C(12)–C(11)	105.74(17)	C(16)–C(12)–C(13)	115.24(18)
C(11)–C(12)–C(13)	114.59(17)	C(15)–C(13)–C(14)	107.78(18)
C(15)–C(13)–C(12)	112.1(2)	C(14)–C(13)–C(12)	113.8(2)
C(17)–C(16)–C(12)	111.96(17)	C(16)–C(17)–C(18)	113.19(18)
C(19)–C(18)–C(17)	108.37(18)	C(19)–C(18)–C(10)	115.93(19)
C(17)–C(18)–C(10)	109.39(17)	

Table 4.   Anisotropic displacement parameters (Å2) for str0165.  The anisotropic
displacement factor exponent takes the form: 2p2[h2a*2U11 + ...+ 2hka*b*U12]

	     U11	     U22	     U33	     U23	     U13	     U12

O(1)	0.0296(8) 	0.0205(7)	0.0194(7) 	 0.0009(6)	0.0003(7) 	 0.0002(6)
O(2)	0.0330(9) 	0.0243(7)	0.0191(7) 	0.0006(6)	 0.0043(7) 	0.0021(6)
C(1)	0.0219(11) 	0.0243(11)	0.0230(10) 	 0.0012(8)	 0.0031(9) 	0.0006(9)
C(2)	0.0172(10) 	0.0308(11)	0.0241(11) 	 0.0053(9)	 0.0002(10) 	0.0006(9)
C(3)	0.0301(13) 	0.0298(11)	0.0296(11) 	 0.0020(9)	 0.0001(10) 	 0.0012(10)
C(4)	0.0358(15) 	0.0363(13)	0.0355(13) 	 0.0134(10)	 0.0030(12) 	0.0000(11)
C(5)	0.0376(14) 	0.0542(16)	0.0257(12) 	 0.0150(11)	 0.0029(12) 	0.0027(13)
C(6)	0.0403(15) 	0.0505(16)	0.0242(12) 	 0.0007(10)	 0.0026(11) 	 0.0007(13)
C(7)	0.0322(14) 	0.0334(12)	0.0262(11) 	0.0006(9)	 0.0022(10) 	0.0016(11)
C(8)	0.0587(17) 	0.0284(11)	0.0286(13) 	0.0042(10)	 0.0080(11) 	0.0036(12)
C(9)	0.0323(13) 	0.0218(10)	0.0200(11) 	0.0011(8)	0.0003(9) 	 0.0067(10)
C(10)	0.0192(10) 	0.0256(10)	0.0184(10) 	0.0002(8)	0.0000(9) 	 0.0042(9)
C(11)	0.0194(10) 	0.0269(11)	0.0192(10) 	 0.0015(8)	0.0004(8) 	0.0040(9)
C(12)	0.0303(12) 	0.0236(10)	0.0235(11) 	0.0006(8)	 0.0016(10) 	0.0081(9)
C(13)	0.0374(13) 	0.0188(10)	0.0356(13) 	0.0036(9)	0.0028(11) 	 0.0011(10)
C(14)	0.0597(18) 	0.0261(12)	0.0462(15) 	0.0025(11)	0.0050(13) 	 0.0128(13)
C(15)	0.0623(18) 	0.0337(13)	0.0445(15) 	0.0003(12)	0.0233(14) 	 0.0074(14)
C(16)	0.0371(13) 	0.0281(11)	0.0318(12) 	 0.0041(10)	0.0053(11) 	0.0084(11)
C(17)	0.0440(15) 	0.0283(11)	0.0244(11) 	 0.0074(9)	0.0058(10) 	0.0032(11)
C(18)	0.0320(13) 	0.0323(12)	0.0219(11) 	 0.0027(9)	0.0056(10) 	 0.0069(10)
C(19)	0.073(2) 	0.0360(13)	0.0185(11) 	 0.0008(9)	0.0003(13) 	 0.0066(14)

Table 5.   Hydrogen coordinates and isotropic displacement parameters (Å2)
for str0165.

	     x 	     y 	     z 	     U

H(1)	0.3054	0.3037	1.0210	0.028
H(3)	0.1586	0.5405	1.0717	0.036
H(4)	0.1227	0.6333	1.1861	0.043
H(5)	0.0993	0.5014	1.2881	0.047
H(6)	0.1180	0.2758	1.2759	0.046
H(7)	0.1556	0.1825	1.1621	0.037
H(8A)	 0.0604	0.3900	0.8686	0.058
H(8B)	0.0732	0.4060	0.8103	0.058
H(8C)	0.0610	0.5050	0.8772	0.058
H(9)	0.2550	0.3473	0.8961	0.030
H(10)	0.0108	0.1600	0.8996	0.025
H(11)	0.3107	0.1203	0.9566	0.026
H(12)	0.2343	 0.0756	1.0040	0.031
H(13)	 0.0639	 0.0137	0.9567	0.037
H(14A)	0.0285	 0.2795	0.9728	0.066
H(14B)	 0.0319	 0.2152	0.8992	0.066
H(14C)	 0.1448	 0.2338	0.9665	0.066
H(15A)	 0.1370	 0.0965	1.0697	0.070
H(15B)	 0.0080	0.0115	1.0807	0.070
H(15C)	0.0340	 0.1397	1.0865	0.070
H(16A)	0.3454	 0.0805	0.8921	0.039
H(16B)	0.2140	 0.1882	0.8904	0.039
H(17A)	0.0538	 0.0470	0.8256	0.039
H(17B)	0.2100	 0.0642	0.7824	0.039
H(18)	0.2974	0.1381	0.8255	0.034
H(19A)	0.1532	0.1229	0.7151	0.064
H(19B)	0.1499	0.2654	0.7501	0.064
H(19C)	0.0067	0.1708	0.7590	0.064

Table 6.  Torsion angles [°] for str0165.

C(11)–O(1)–C(1)–O(2)	65.9(2)	C(11)–O(1)–C(1)–C(2)	 174.65(15)
C(9)–O(2)–C(1)–O(1)	 64.9(2)	C(9)–O(2)–C(1)–C(2)	174.55(16)
O(1)–C(1)–C(2)–C(7)	21.8(3)	O(2)–C(1)–C(2)–C(7)	142.6(2)
O(1)–C(1)–C(2)–C(3)	 161.17(19)	O(2)–C(1)–C(2)–C(3)	 40.3(3)
C(7)–C(2)–C(3)–C(4)	0.5(4)	C(1)–C(2)–C(3)–C(4)	 176.6(2)
C(2)–C(3)–C(4)–C(5)	 0.7(4)	C(3)–C(4)–C(5)–C(6)	0.7(4)
C(4)–C(5)–C(6)–C(7)	 0.5(4)	C(3)–C(2)–C(7)–C(6)	 0.3(4)
C(1)–C(2)–C(7)–C(6)	176.7(2)	C(5)–C(6)–C(7)–C(2)	0.3(4)
C(1)–O(2)–C(9)–C(8)	 179.48(17)	C(1)–O(2)–C(9)–C(10)	55.1(2)
O(2)–C(9)–C(10)–C(11)	 47.2(2)	C(8)–C(9)–C(10)–C(11)	 163.93(19)
O(2)–C(9)–C(10)–C(18)	 168.56(17)	C(8)–C(9)–C(10)–C(18)	74.7(3)
C(1)–O(1)–C(11)–C(12)	173.54(16)	C(1)–O(1)–C(11)–C(10)	 59.3(2)
C(18)–C(10)–C(11)–O(1)	175.47(15)	C(9)–C(10)–C(11)–O(1)	50.2(2)
C(18)–C(10)–C(11)–C(12)	 60.6(2)	C(9)–C(10)–C(11)–C(12)	174.08(17)
O(1)–C(11)–C(12)–C(16)	 174.77(16)	C(10)–C(11)–C(12)–C(16)	60.1(2)
O(1)–C(11)–C(12)–C(13)	57.2(2)	C(10)–C(11)–C(12)–C(13)	 68.0(2)
C(16)–C(12)–C(13)–C(15)	154.94(19)	C(11)–C(12)–C(13)–C(15)	 82.0(2)
C(16)–C(12)–C(13)–C(14)	32.3(3)	C(11)–C(12)–C(13)–C(14)	155.35(19)
C(11)–C(12)–C(16)–C(17)	 56.2(2)	C(13)–C(12)–C(16)–C(17)	71.5(2)
C(12)–C(16)–C(17)–C(18)	57.6(3)	C(16)–C(17)–C(18)–C(19)	177.32(19)
C(16)–C(17)–C(18)–C(10)	 55.4(3)	C(11)–C(10)–C(18)–C(19)	177.37(18)
C(9)–C(10)–C(18)–C(19)	 60.8(3)	C(11)–C(10)–C(18)–C(17)	54.5(2)
C(9)–C(10)–C(18)–C(17)	176.36(19)	

Table 1.  Crystal data and structure refinement for str58.

Identification code 	str0166
Chemical formula 	C19H28O2
Formula weight 	288.41
Temperature 	293(2) K
Radiation, wavelength 	MoKa, 0.71073 Å
Crystal system, space group 	orthorhombic, P212121
Unit cell parameters	a = 8.5195(11) Å	a = 90°
	b = 10.0386(13) Å	b = 90°
	c = 19.370(2) Å	g = 90°
Cell volume	1656.6(4) Å3
Z	4
Calculated density 	1.156 g/cm3
Absorption coefficient m	0.073 mm-1
F(000)	632
Crystal colour and size	colourless, 0.50 ´ 0.10 ´ 0.08 mm3
Data collection method	Bruker SMART APEX diffractometer
	w rotation with narrow frames
q range for data collection	2.10 to 28.26°
Index ranges	h -11 to 11, k -13 to 13, l -24 to 25
Completeness to q = 26.00°	99.8 % 
Reflections collected	14785
Independent reflections	3974 (Rint = 0.0391)
Reflections with F2>2s	3275
Absorption correction	semi-empirical from equivalents
Min. and max. transmission	0.9646 and 0.9942
Structure solution	direct methods
Refinement method	Full-matrix least-squares on F2
Weighting parameters a, b	0.0606, 0.0651
Data / restraints / parameters	3974 / 0 / 195
Final R indices [F2>2s]	R1 = 0.0535, wR2 = 0.1178
R indices (all data)	R1 = 0.0682, wR2 = 0.1251
Goodness-of-fit on F2	1.070
Extinction coefficient	0.019(3)
Largest and mean shift/su	0.001 and 0.000
Largest diff. peak and hole	0.171 and -0.196 e Å-3

Table 2.  Atomic coordinates and equivalent isotropic displacement parameters (Å2)
for str0166.  Ueq is defined as one third of the trace of the orthogonalized Uij tensor.

	     x	     y	     z	     Ueq

O(1)	0.09853(12)	0.15854(11)	1.01911(5)	0.0363(3)
O(2)	0.12026(14)	0.36812(11)	0.97244(5)	0.0423(3)
C(1)	0.1739(2)	0.28297(16)	1.02415(8)	0.0364(4)
C(2)	0.14091(19)	0.34320(17)	1.09380(8)	0.0375(4)
C(3)	0.1198(2)	0.47872(18)	1.10138(9)	0.0470(5)
C(4)	0.0985(2)	0.5341(2)	1.16628(10)	0.0581(5)
C(5)	0.0986(3)	0.4559(2)	1.22370(10)	0.0591(6)
C(6)	0.1196(3)	0.3209(2)	1.21706(10)	0.0582(5)
C(7)	0.1408(2)	0.2644(2)	1.15244(9)	0.0487(4)
C(8)	0.0925(3)	0.4280(2)	0.85756(9)	0.0586(6)
C(9)	0.1634(2)	0.32299(18)	0.90452(8)	0.0409(4)
C(10)	0.1053(2)	0.17975(17)	0.89320(8)	0.0380(4)
C(11)	0.14647(19)	0.09394(16)	0.95619(8)	0.0347(4)
C(12)	0.0720(2)	 -0.04398(17)	0.95364(9)	0.0408(4)
C(13)	0.0970(2)	 -0.13141(17)	1.01822(9)	0.0484(5)
C(14)	0.2634(3)	 -0.1242(2)	1.04711(11)	0.0672(6)
C(15)	 -0.0238(3)	 -0.1050(2)	1.07436(10)	0.0656(6)
C(16)	0.1335(3)	 -0.11318(19)	0.88864(9)	0.0551(5)
C(17)	0.1050(3)	 -0.0312(2)	0.82429(9)	0.0589(6)
C(18)	0.1724(2)	0.1098(2)	0.82857(8)	0.0485(5)
C(19)	0.1446(3)	0.1794(3)	0.75959(10)	0.0806(8)

Table 3.   Bond lengths [Å] and angles [°] for str0166.

O(1)-C(1) 	1.4079(19)	O(1)-C(11) 	1.4397(18)
O(2)-C(1) 	1.3939(19)	O(2)-C(9) 	1.4392(19)
C(1)-C(2) 	1.505(2)	C(2)-C(3) 	1.380(3)
C(2)-C(7) 	1.384(2)	C(3)-C(4) 	1.386(3)
C(4)-C(5) 	1.362(3)	C(5)-C(6) 	1.373(3)
C(6)-C(7) 	1.386(3)	C(8)-C(9) 	1.518(2)
C(9)-C(10) 	1.537(2)	C(10)-C(11) 	1.534(2)
C(10)-C(18) 	1.545(2)	C(11)-C(12) 	1.524(2)
C(12)-C(16) 	1.530(2)	C(12)-C(13) 	1.543(2)
C(13)-C(15) 	1.521(3)	C(13)-C(14) 	1.526(3)
C(16)-C(17) 	1.513(3)	C(17)-C(18) 	1.530(3)
C(18)-C(19) 	1.526(3)	

C(1)-O(1)-C(11)	109.20(11)	C(1)-O(2)-C(9)	112.33(12)
O(2)-C(1)-O(1)	110.16(13)	O(2)-C(1)-C(2)	109.66(13)
O(1)-C(1)-C(2)	109.48(13)	C(3)-C(2)-C(7)	118.44(16)
C(3)-C(2)-C(1)	121.05(16)	C(7)-C(2)-C(1)	120.40(16)
C(2)-C(3)-C(4)	120.59(18)	C(5)-C(4)-C(3)	120.61(18)
C(4)-C(5)-C(6)	119.53(18)	C(5)-C(6)-C(7)	120.37(19)
C(2)-C(7)-C(6)	120.47(18)	O(2)-C(9)-C(8)	103.16(14)
O(2)-C(9)-C(10)	110.04(13)	C(8)-C(9)-C(10)	115.85(15)
C(11)-C(10)-C(9)	109.77(13)	C(11)-C(10)-C(18)	107.73(14)
C(9)-C(10)-C(18)	114.95(15)	O(1)-C(11)-C(12)	108.58(12)
O(1)-C(11)-C(10)	110.82(12)	C(12)-C(11)-C(10)	112.90(13)
C(11)-C(12)-C(16)	107.26(14)	C(11)-C(12)-C(13)	115.67(14)
C(16)-C(12)-C(13)	111.20(14)	C(15)-C(13)-C(14)	111.00(17)
C(15)-C(13)-C(12)	112.78(15)	C(14)-C(13)-C(12)	113.49(16)
C(17)-C(16)-C(12)	112.08(16)	C(16)-C(17)-C(18)	113.46(16)
C(19)-C(18)-C(17)	108.55(16)	C(19)-C(18)-C(10)	116.36(17)
C(17)-C(18)-C(10)	109.01(15)	

Table 4.   Anisotropic displacement parameters (Å2) for str0166.  The anisotropic
displacement factor exponent takes the form: -2p2[h2a*2U11 + ...+ 2hka*b*U12]

	     U11	     U22	     U33	     U23	     U13	     U12

O(1)	0.0419(6) 	0.0358(6)	0.0313(6) 	 -0.0010(4)	0.0025(5) 	 -0.0035(5)
O(2)	0.0559(7) 	0.0381(6)	0.0331(6) 	0.0010(5)	0.0009(5) 	0.0011(6)
C(1)	0.0344(9) 	0.0375(9)	0.0372(9) 	 -0.0005(7)	 -0.0011(7) 	 -0.0017(7)
C(2)	0.0337(8) 	0.0423(9)	0.0367(8) 	 -0.0034(7)	 -0.0024(7) 	 -0.0030(8)
C(3)	0.0547(11) 	0.0434(10)	0.0428(10) 	 -0.0027(8)	 -0.0039(9) 	 -0.0028(9)
C(4)	0.0663(14) 	0.0513(11)	0.0568(12) 	 -0.0168(9)	 -0.0005(10) 	 -0.0017(10)
C(5)	0.0647(14) 	0.0718(14)	0.0407(10) 	 -0.0178(10)	 -0.0008(10) 	 -0.0056(11)
C(6)	0.0687(14) 	0.0714(14)	0.0344(9) 	0.0029(9)	0.0000(9) 	 -0.0029(12)
C(7)	0.0568(12) 	0.0481(10)	0.0411(9) 	 -0.0009(8)	 -0.0002(9) 	 -0.0001(10)
C(8)	0.0827(15) 	0.0516(11)	0.0415(10) 	0.0095(9)	0.0013(11) 	0.0095(11)
C(9)	0.0440(10) 	0.0449(9)	0.0336(9) 	0.0029(7)	0.0041(7) 	 -0.0018(8)
C(10)	0.0336(8) 	0.0469(9)	0.0336(8) 	0.0006(7)	0.0016(7) 	0.0012(8)
C(11)	0.0338(8) 	0.0371(8)	0.0331(8) 	 -0.0019(7)	0.0008(7) 	0.0012(7)
C(12)	0.0402(9) 	0.0388(9)	0.0434(9) 	 -0.0036(7)	 -0.0010(8) 	 -0.0014(7)
C(13)	0.0622(12) 	0.0325(9)	0.0506(10) 	 -0.0007(8)	0.0010(9) 	 -0.0011(9)
C(14)	0.0770(14) 	0.0623(14)	0.0622(13) 	0.0095(11)	 -0.0149(11) 	0.0141(12)
C(15)	0.0834(16) 	0.0547(12)	0.0587(12) 	0.0090(11)	0.0183(11) 	 -0.0050(12)
C(16)	0.0739(14) 	0.0426(10)	0.0489(10) 	 -0.0122(8)	 -0.0018(10) 	0.0001(11)
C(17)	0.0729(14) 	0.0608(12)	0.0429(10) 	 -0.0178(9)	0.0024(10) 	0.0005(11)
C(18)	0.0503(10) 	0.0586(11)	0.0365(9) 	 -0.0052(8)	0.0059(8) 	 -0.0017(10)
C(19)	0.132(2) 	0.0743(15)	0.0352(11) 	 -0.0015(10)	0.0114(13) 	 -0.0022(17)

Table 5.   Hydrogen coordinates and isotropic displacement parameters (Å2)
for str0166.

	     x 	     y 	     z 	     U

H(1)	0.2874	0.2704	1.0189	0.044
H(3)	0.1198	0.5334	1.0626	0.056
H(4)	0.0841	0.6256	1.1706	0.070
H(5)	0.0845	0.4936	1.2671	0.071
H(6)	0.1195	0.2670	1.2561	0.070
H(7)	0.1551	0.1728	1.1485	0.058
H(8A)	 -0.0193	0.4164	0.8557	0.088
H(8B)	0.1355	0.4189	0.8120	0.088
H(8C)	0.1163	0.5150	0.8753	0.088
H(9)	0.2780	0.3251	0.9000	0.049
H(10)	 -0.0093	0.1822	0.8889	0.046
H(11)	0.2607	0.0829	0.9575	0.042
H(12)	 -0.0413	 -0.0317	0.9478	0.049
H(13)	0.0811	 -0.2237	1.0034	0.058
H(14A)	0.2804	 -0.0382	1.0674	0.101
H(14B)	0.3375	 -0.1380	1.0105	0.101
H(14C)	0.2770	 -0.1919	1.0816	0.101
H(15A)	 -0.0079	 -0.0174	1.0930	0.098
H(15B)	 -0.0124	 -0.1699	1.1104	0.098
H(15C)	 -0.1274	 -0.1110	1.0551	0.098
H(16A)	0.2453	 -0.1290	0.8936	0.066
H(16B)	0.0821	 -0.1989	0.8837	0.066
H(17A)	 -0.0072	 -0.0255	0.8162	0.071
H(17B)	0.1515	 -0.0766	0.7851	0.071
H(18)	0.2861	0.1017	0.8349	0.058
H(19A)	0.1726	0.1204	0.7226	0.121
H(19B)	0.2080	0.2583	0.7572	0.121
H(19C)	0.0359	0.2032	0.7556	0.121

Table 6.  Torsion angles [°] for str0166.

C(9)-O(2)-C(1)-O(1)	 -65.71(17)	C(9)-O(2)-C(1)-C(2)	173.73(13)
C(11)-O(1)-C(1)-O(2)	66.58(15)	C(11)-O(1)-C(1)-C(2)	 -172.75(13)
O(2)-C(1)-C(2)-C(3)	 -22.7(2)	O(1)-C(1)-C(2)-C(3)	 -143.64(17)
O(2)-C(1)-C(2)-C(7)	161.37(16)	O(1)-C(1)-C(2)-C(7)	40.4(2)
C(7)-C(2)-C(3)-C(4)	 -0.2(3)	C(1)-C(2)-C(3)-C(4)	 -176.22(16)
C(2)-C(3)-C(4)-C(5)	0.2(3)	C(3)-C(4)-C(5)-C(6)	 -0.1(4)
C(4)-C(5)-C(6)-C(7)	0.1(4)	C(3)-C(2)-C(7)-C(6)	0.1(3)
C(1)-C(2)-C(7)-C(6)	176.21(18)	C(5)-C(6)-C(7)-C(2)	 -0.1(3)
C(1)-O(2)-C(9)-C(8)	179.38(14)	C(1)-O(2)-C(9)-C(10)	55.20(18)
O(2)-C(9)-C(10)-C(11)	 -46.58(19)	C(8)-C(9)-C(10)-C(11)	 -163.06(15)
O(2)-C(9)-C(10)-C(18)	 -168.18(14)	C(8)-C(9)-C(10)-C(18)	75.3(2)
C(1)-O(1)-C(11)-C(12)	176.52(13)	C(1)-O(1)-C(11)-C(10)	 -58.93(16)
C(9)-C(10)-C(11)-O(1)	49.52(18)	C(18)-C(10)-C(11)-O(1)	175.35(13)
C(9)-C(10)-C(11)-C(12)	171.57(13)	C(18)-C(10)-C(11)-C(12)	 -62.59(18)
O(1)-C(11)-C(12)-C(16)	 -176.44(13)	C(10)-C(11)-C(12)-C(16)	60.25(18)
O(1)-C(11)-C(12)-C(13)	 -51.73(18)	C(10)-C(11)-C(12)-C(13)	 -175.04(14)
C(11)-C(12)-C(13)-C(15)	85.32(19)	C(16)-C(12)-C(13)-C(15)	 -152.03(18)
C(11)-C(12)-C(13)-C(14)	 -42.0(2)	C(16)-C(12)-C(13)-C(14)	80.6(2)
C(11)-C(12)-C(16)-C(17)	 -54.7(2)	C(13)-C(12)-C(16)-C(17)	177.97(16)
C(12)-C(16)-C(17)-C(18)	55.1(2)	C(16)-C(17)-C(18)-C(19)	176.79(18)
C(16)-C(17)-C(18)-C(10)	 -55.6(2)	C(11)-C(10)-C(18)-C(19)	 -179.84(17)
C(9)-C(10)-C(18)-C(19)	 -57.1(2)	C(11)-C(10)-C(18)-C(17)	57.05(19)
C(9)-C(10)-C(18)-C(17)	179.76(15)	

Table 1.  Crystal data and structure refinement for structure 30

Identification code 	str0154
Chemical formula 	C34H42O4
Formula weight 	514.68
Temperature 	293(2) K
Radiation, wavelength 	MoKa, 0.71073 Å
Crystal system, space group 	orthorhombic, P212121
Unit cell parameters	a = 10.6743(7) Å	a = 90°
	b = 16.4346(10) Å	b = 90°
	c = 16.6813(10) Å	g = 90°
Cell volume	2926.4(3) Å3
Z	4
Calculated density 	1.168 g/cm3
Absorption coefficient m	0.075 mm1
F(000)	1112
Crystal colour and size	colourless, 0.48  0.48  0.08 mm3
Data collection method	Bruker SMART APEX diffractometer
	w rotation with narrow frames
q range for data collection	1.74 to 28.33°
Index ranges	h 14 to 14, k 21 to 21, l 21 to 20
Completeness to q = 26.00°	99.9 % 
Reflections collected	26059
Independent reflections	6887 (Rint = 0.0313)
Reflections with F2>2s	5908
Absorption correction	semi-empirical from equivalents
Min. and max. transmission	0.9650 and 0.9940
Structure solution	direct methods
Refinement method	Full-matrix least-squares on F2
Weighting parameters a, b	0.0634, 0.1579
Data / restraints / parameters	6887 / 0 / 349
Final R indices [F2>2s]	R1 = 0.0426, wR2 = 0.1077
R indices (all data)	R1 = 0.0507, wR2 = 0.1136
Goodness-of-fit on F2	1.015
Absolute structure parameter	0.1(8)
Largest and mean shift/su	0.000 and 0.000
Largest diff. peak and hole	0.134 and 0.185 e Å3

Table 2.  Atomic coordinates and equivalent isotropic displacement parameters (Å2)
for str0154.  Ueq is defined as one third of the trace of the orthogonalized Uij tensor.

	     x	     y	     z	     Ueq

O(1)	0.32379(9)	0.56017(7)	0.00712(6)	0.0535(2)
O(2)	0.11248(9)	0.57868(6)	0.01045(6)	0.0490(2)
O(3)	0.19957(10)	0.41654(6)	0.01927(6)	0.0536(2)
O(4)	0.30473(9)	0.44746(6)	0.13393(6)	0.0515(2)
C(1)	0.2454(3)	0.88622(12)	 0.00699(15)	0.0971(7)
C(2)	0.2471(2)	0.83880(13)	 0.15014(12)	0.0805(6)
C(3)	0.24096(19)	0.81439(10)	 0.06370(11)	0.0669(4)
C(4)	0.30344(17)	0.73774(10)	 0.03230(10)	0.0610(4)
C(5)	0.16191(16)	0.74401(10)	 0.03513(10)	0.0582(4)
C(6)	0.10151(16)	0.68261(11)	 0.08961(10)	0.0599(4)
C(7)	0.14780(15)	0.59718(10)	 0.07111(9)	0.0522(3)
C(8)	0.29204(14)	0.59141(9)	 0.06993(8)	0.0515(3)
C(9)	0.35681(16)	0.67218(11)	 0.08487(12)	0.0642(4)
C(10)	0.0888(2)	0.53462(12)	 0.12661(10)	0.0742(5)
C(11)	0.21733(13)	0.55813(8)	0.05732(8)	0.0455(3)
C(12)	0.23424(16)	0.61671(9)	0.12679(9)	0.0518(3)
C(13)	0.13393(19)	0.66122(10)	0.15566(10)	0.0651(4)
C(14)	0.1524(3)	0.71669(12)	0.21737(13)	0.0858(7)
C(15)	0.2689(3)	0.72632(13)	0.25088(13)	0.0961(8)
C(16)	0.3677(3)	0.68205(14)	0.22296(13)	0.0906(7)
C(17)	0.3517(2)	0.62685(11)	0.16050(11)	0.0703(5)
C(18)	0.3238(2)	0.12460(12)	0.10234(14)	0.0885(6)
C(19)	0.0970(3)	0.13620(13)	0.13997(14)	0.0896(7)
C(20)	0.21266(19)	0.18014(10)	0.11155(10)	0.0627(4)
C(21)	0.18930(16)	0.25134(9)	0.05636(9)	0.0557(4)
C(22)	0.22778(17)	0.26607(9)	0.14232(9)	0.0559(4)
C(23)	0.35418(18)	0.30535(10)	0.15199(11)	0.0664(5)
C(24)	0.37232(14)	0.38067(10)	0.09927(10)	0.0545(4)
C(25)	0.31360(15)	0.37086(10)	0.01590(9)	0.0555(4)
C(26)	0.27960(18)	0.28331(10)	 0.00465(10)	0.0622(4)
C(27)	0.50903(16)	0.40506(14)	0.09538(16)	0.0852(6)
C(28)	0.20019(12)	0.46803(8)	0.08672(8)	0.0446(3)
C(29)	0.07941(13)	0.45634(8)	0.13346(8)	0.0462(3)
C(30)	 0.03027(15)	0.43920(11)	0.09320(11)	0.0632(4)
C(31)	 0.14009(18)	0.42723(13)	0.13528(14)	0.0789(5)
C(32)	 0.14038(18)	0.43205(12)	0.21748(14)	0.0758(5)
C(33)	 0.03226(18)	0.44940(11)	0.25748(11)	0.0694(5)
C(34)	0.07838(16)	0.46162(10)	0.21569(9)	0.0578(4)

Table 3.   Bond lengths [Å] and angles [°] for str0154.

O(1)–C(11) 	1.4120(17)	O(1)–C(8) 	1.4248(18)
O(2)–C(11) 	1.4064(17)	O(2)–C(7) 	1.4442(18)
O(3)–C(28) 	1.4079(16)	O(3)–C(25) 	1.4312(19)
O(4)–C(28) 	1.4071(16)	O(4)–C(24) 	1.4352(18)
C(1)–C(3) 	1.513(3)	C(2)–C(3) 	1.498(3)
C(3)–C(5) 	1.509(2)	C(3)–C(4) 	1.519(2)
C(4)–C(9) 	1.501(2)	C(4)–C(5) 	1.515(2)
C(5)–C(6) 	1.503(2)	C(6)–C(7) 	1.520(2)
C(7)–C(10) 	1.520(2)	C(7)–C(8) 	1.543(2)
C(8)–C(9) 	1.517(2)	C(11)–C(12) 	1.517(2)
C(11)–C(28) 	1.5704(19)	C(12)–C(17) 	1.384(3)
C(12)–C(13) 	1.383(2)	C(13)–C(14) 	1.389(3)
C(14)–C(15) 	1.373(4)	C(15)–C(16) 	1.363(4)
C(16)–C(17) 	1.392(3)	C(18)–C(20) 	1.505(3)
C(19)–C(20) 	1.507(3)	C(20)–C(21) 	1.510(2)
C(20)–C(22) 	1.511(2)	C(21)–C(26) 	1.497(2)
C(21)–C(22) 	1.511(2)	C(22)–C(23) 	1.504(3)
C(23)–C(24) 	1.531(2)	C(24)–C(27) 	1.515(2)
C(24)–C(25) 	1.534(2)	C(25)–C(26) 	1.523(2)
C(28)–C(29) 	1.5189(19)	C(29)–C(34) 	1.374(2)
C(29)–C(30) 	1.379(2)	C(30)–C(31) 	1.380(3)
C(31)–C(32) 	1.373(3)	C(32)–C(33) 	1.363(3)
C(33)–C(34) 	1.386(2)	

C(11)–O(1)–C(8)	110.61(10)	C(11)–O(2)–C(7)	111.50(10)
C(28)–O(3)–C(25)	110.04(10)	C(28)–O(4)–C(24)	110.91(11)
C(2)–C(3)–C(5)	122.25(17)	C(2)–C(3)–C(1)	113.04(17)
C(5)–C(3)–C(1)	114.72(17)	C(2)–C(3)–C(4)	122.33(18)
C(5)–C(3)–C(4)	60.05(11)	C(1)–C(3)–C(4)	114.69(17)
C(9)–C(4)–C(5)	114.14(14)	C(9)–C(4)–C(3)	124.09(15)
C(5)–C(4)–C(3)	59.66(11)	C(6)–C(5)–C(3)	124.30(15)
C(6)–C(5)–C(4)	113.64(14)	C(3)–C(5)–C(4)	60.29(12)
C(5)–C(6)–C(7)	110.97(13)	O(2)–C(7)–C(6)	107.51(13)
O(2)–C(7)–C(10)	108.85(12)	C(6)–C(7)–C(10)	111.49(14)
O(2)–C(7)–C(8)	103.62(12)	C(6)–C(7)–C(8)	112.57(13)
C(10)–C(7)–C(8)	112.33(15)	O(1)–C(8)–C(9)	110.80(13)
O(1)–C(8)–C(7)	105.73(11)	C(9)–C(8)–C(7)	113.51(14)
C(4)–C(9)–C(8)	111.04(13)	O(2)–C(11)–O(1)	107.76(11)
O(2)–C(11)–C(12)	111.52(12)	O(1)–C(11)–C(12)	110.01(11)
O(2)–C(11)–C(28)	107.90(11)	O(1)–C(11)–C(28)	107.54(11)
C(12)–C(11)–C(28)	111.93(11)	C(17)–C(12)–C(13)	119.73(15)
C(17)–C(12)–C(11)	119.64(15)	C(13)–C(12)–C(11)	120.62(15)
C(12)–C(13)–C(14)	119.7(2)	C(15)–C(14)–C(13)	120.4(2)
C(16)–C(15)–C(14)	120.01(19)	C(15)–C(16)–C(17)	120.6(2)
C(12)–C(17)–C(16)	119.6(2)	C(18)–C(20)–C(19)	112.80(17)
C(18)–C(20)–C(21)	122.55(17)	C(19)–C(20)–C(21)	115.34(18)
C(18)–C(20)–C(22)	121.15(18)	C(19)–C(20)–C(22)	115.37(16)
C(21)–C(20)–C(22)	60.03(10)	C(26)–C(21)–C(20)	125.47(16)
C(26)–C(21)–C(22)	114.45(14)	C(20)–C(21)–C(22)	60.04(10)
C(23)–C(22)–C(20)	122.22(15)	C(23)–C(22)–C(21)	114.48(14)
C(20)–C(22)–C(21)	59.93(10)	C(22)–C(23)–C(24)	113.50(13)
O(4)–C(24)–C(27)	107.40(14)	O(4)–C(24)–C(23)	108.87(13)
C(27)–C(24)–C(23)	111.13(16)	O(4)–C(24)–C(25)	103.90(12)
C(27)–C(24)–C(25)	112.50(16)	C(23)–C(24)–C(25)	112.59(13)
O(3)–C(25)–C(26)	107.56(13)	O(3)–C(25)–C(24)	104.88(11)
C(26)–C(25)–C(24)	113.63(14)	C(21)–C(26)–C(25)	109.39(13)
O(4)–C(28)–O(3)	107.85(10)	O(4)–C(28)–C(29)	110.82(10)
O(3)–C(28)–C(29)	109.28(11)	O(4)–C(28)–C(11)	108.00(11)
O(3)–C(28)–C(11)	108.52(11)	C(29)–C(28)–C(11)	112.24(11)
C(34)–C(29)–C(30)	119.49(15)	C(34)–C(29)–C(28)	120.74(13)
C(30)–C(29)–C(28)	119.77(13)	C(29)–C(30)–C(31)	120.16(17)
C(32)–C(31)–C(30)	120.09(18)	C(33)–C(32)–C(31)	119.92(17)
C(32)–C(33)–C(34)	120.36(17)	C(29)–C(34)–C(33)	119.98(16)

Table 4.   Anisotropic displacement parameters (Å2) for str0154.  The anisotropic
displacement factor exponent takes the form: 2p2[h2a*2U11 + ...+ 2hka*b*U12]

	     U11	     U22	     U33	     U23	     U13	     U12

O(1)	0.0448(5) 	0.0664(6)	0.0492(5) 	0.0022(5)	0.0032(4) 	 0.0030(4)
O(2)	0.0445(5) 	0.0544(6)	0.0482(5) 	0.0096(4)	0.0002(4) 	 0.0023(4)
O(3)	0.0601(6) 	0.0524(6)	0.0482(5) 	 0.0087(4)	 0.0067(5) 	0.0044(5)
O(4)	0.0509(5) 	0.0538(6)	0.0499(5) 	 0.0077(4)	 0.0079(4) 	0.0095(4)
C(1)	0.138(2) 	0.0543(10)	0.0986(15) 	 0.0023(11)	 0.0053(15) 	 0.0004(12)
C(2)	0.0850(13) 	0.0744(12)	0.0822(13) 	0.0255(10)	0.0063(11) 	 0.0112(11)
C(3)	0.0771(11) 	0.0507(8)	0.0728(10) 	0.0082(8)	 0.0003(9) 	 0.0056(8)
C(4)	0.0654(10) 	0.0506(8)	0.0669(9) 	0.0034(7)	 0.0067(8) 	 0.0097(7)
C(5)	0.0661(10) 	0.0519(8)	0.0567(8) 	0.0089(7)	0.0080(7) 	0.0025(7)
C(6)	0.0534(8) 	0.0668(10)	0.0596(9) 	0.0173(8)	 0.0042(7) 	 0.0052(7)
C(7)	0.0550(8) 	0.0573(8)	0.0444(7) 	0.0054(6)	 0.0020(6) 	 0.0123(7)
C(8)	0.0560(8) 	0.0535(8)	0.0450(7) 	 0.0030(6)	0.0071(6) 	 0.0021(7)
C(9)	0.0540(9) 	0.0626(10)	0.0760(11) 	0.0065(9)	0.0119(8) 	 0.0094(8)
C(10)	0.0852(12) 	0.0780(12)	0.0594(9) 	 0.0011(9)	 0.0116(9) 	 0.0242(10)
C(11)	0.0413(6) 	0.0481(7)	0.0472(7) 	0.0001(6)	0.0008(5) 	 0.0014(6)
C(12)	0.0638(9) 	0.0445(7)	0.0469(7) 	0.0017(6)	0.0031(7) 	 0.0065(7)
C(13)	0.0780(11) 	0.0553(9)	0.0621(10) 	 0.0022(7)	0.0173(9) 	 0.0018(8)
C(14)	0.1251(19) 	0.0634(11)	0.0688(12) 	 0.0117(9)	0.0292(13) 	 0.0014(12)
C(15)	0.163(2) 	0.0660(12)	0.0595(11) 	 0.0164(9)	 0.0052(14) 	 0.0097(15)
C(16)	0.1214(19) 	0.0733(12)	0.0770(13) 	 0.0142(11)	 0.0304(13) 	 0.0152(13)
C(17)	0.0797(12) 	0.0641(10)	0.0672(10) 	 0.0107(8)	 0.0158(9) 	 0.0026(9)
C(18)	0.1155(18) 	0.0592(10)	0.0907(13) 	 0.0091(10)	 0.0034(13) 	0.0254(11)
C(19)	0.1140(18) 	0.0703(12)	0.0846(13) 	0.0017(11)	0.0011(13) 	 0.0265(12)
C(20)	0.0818(11) 	0.0487(8)	0.0575(9) 	 0.0044(7)	 0.0016(8) 	0.0022(8)
C(21)	0.0625(9) 	0.0509(8)	0.0538(8) 	 0.0079(6)	 0.0036(7) 	0.0012(7)
C(22)	0.0708(10) 	0.0505(8)	0.0464(7) 	 0.0037(6)	0.0020(7) 	0.0066(7)
C(23)	0.0772(11) 	0.0564(9)	0.0655(10) 	 0.0032(8)	 0.0244(9) 	0.0080(8)
C(24)	0.0448(7) 	0.0548(8)	0.0640(9) 	 0.0085(7)	 0.0011(7) 	0.0060(6)
C(25)	0.0594(9) 	0.0549(8)	0.0522(8) 	 0.0045(6)	0.0104(7) 	0.0035(7)
C(26)	0.0812(11) 	0.0567(8)	0.0486(8) 	 0.0104(7)	0.0056(8) 	0.0071(8)
C(27)	0.0461(9) 	0.0968(15)	0.1128(16) 	 0.0289(13)	0.0050(10) 	 0.0027(9)
C(28)	0.0466(7) 	0.0451(7)	0.0420(6) 	 0.0030(5)	 0.0047(6) 	0.0011(6)
C(29)	0.0493(7) 	0.0372(6)	0.0520(7) 	0.0043(6)	 0.0004(6) 	0.0013(6)
C(30)	0.0549(8) 	0.0697(10)	0.0650(9) 	0.0089(8)	 0.0046(7) 	 0.0118(8)
C(31)	0.0519(9) 	0.0840(13)	0.1009(15) 	0.0163(12)	 0.0018(9) 	 0.0132(9)
C(32)	0.0635(10) 	0.0642(10)	0.0998(14) 	0.0203(10)	0.0260(10) 	0.0028(9)
C(33)	0.0788(12) 	0.0638(10)	0.0656(10) 	0.0091(8)	0.0185(9) 	0.0115(9)
C(34)	0.0584(9) 	0.0615(9)	0.0535(8) 	0.0015(7)	0.0024(7) 	0.0068(7)

Table 5.   Hydrogen coordinates and isotropic displacement parameters (Å2)
for str0154.

	     x 	     y 	     z 	     U

H(1A)	0.1756	0.9215	 0.0175	0.146
H(1B)	0.3222	0.9156	 0.0149	0.146
H(1C)	0.2412	0.8671	0.0473	0.146
H(2A)	0.2541	0.7910	 0.1830	0.121
H(2B)	0.3188	0.8730	 0.1586	0.121
H(2C)	0.1724	0.8680	 0.1643	0.121
H(4)	0.3409	0.7422	0.0211	0.073
H(5)	0.1206	0.7518	0.0168	0.070
H(6A)	0.1207	0.6959	 0.1449	0.072
H(6B)	0.0113	0.6847	 0.0830	0.072
H(8)	0.3190	0.5524	 0.1109	0.062
H(9A)	0.4457	0.6666	 0.0742	0.077
H(9B)	0.3467	0.6874	 0.1407	0.077
H(10A)	0.1156	0.4811	 0.1112	0.111
H(10B)	0.1143	0.5452	 0.1808	0.111
H(10C)	 0.0008	0.5380	 0.1228	0.111
H(13)	0.0545	0.6540	0.1339	0.078
H(14)	0.0854	0.7475	0.2361	0.103
H(15)	0.2805	0.7630	0.2926	0.115
H(16)	0.4465	0.6888	0.2458	0.109
H(17)	0.4195	0.5970	0.1415	0.084
H(18A)	0.3932	0.1547	0.0809	0.133
H(18B)	0.3029	0.0809	0.0666	0.133
H(18C)	0.3463	0.1027	0.1537	0.133
H(19A)	0.1121	0.1136	0.1922	0.134
H(19B)	0.0770	0.0932	0.1031	0.134
H(19C)	0.0282	0.1738	0.1427	0.134
H(21)	0.1009	0.2622	0.0447	0.067
H(22)	0.1618	0.2857	0.1783	0.067
H(23A)	0.4185	0.2658	0.1389	0.080
H(23B)	0.3652	0.3208	0.2077	0.080
H(25)	0.3694	0.3934	 0.0251	0.067
H(26A)	0.2420	0.2811	 0.0575	0.075
H(26B)	0.3546	0.2500	 0.0051	0.075
H(27A)	0.5167	0.4558	0.0673	0.128
H(27B)	0.5557	0.3638	0.0676	0.128
H(27C)	0.5413	0.4110	0.1488	0.128
H(30)	 0.0303	0.4357	0.0376	0.076
H(31)	 0.2140	0.4159	0.1079	0.095
H(32)	 0.2142	0.4235	0.2458	0.091
H(33)	 0.0327	0.4531	0.3131	0.083
H(34)	0.1519	0.4734	0.2433	0.069

Table 6.  Torsion angles [°] for str0154.

C(2)–C(3)–C(4)–C(9)	 11.2(3)	C(5)–C(3)–C(4)–C(9)	100.14(18)
C(1)–C(3)–C(4)–C(9)	 154.42(18)	C(2)–C(3)–C(4)–C(5)	 111.4(2)
C(1)–C(3)–C(4)–C(5)	105.44(19)	C(2)–C(3)–C(5)–C(6)	11.7(3)
C(1)–C(3)–C(5)–C(6)	154.85(18)	C(4)–C(3)–C(5)–C(6)	 99.76(18)
C(2)–C(3)–C(5)–C(4)	111.5(2)	C(1)–C(3)–C(5)–C(4)	 105.39(19)
C(9)–C(4)–C(5)–C(6)	0.6(2)	C(3)–C(4)–C(5)–C(6)	117.29(16)
C(9)–C(4)–C(5)–C(3)	 116.71(17)	C(3)–C(5)–C(6)–C(7)	120.26(18)
C(4)–C(5)–C(6)–C(7)	51.13(18)	C(11)–O(2)–C(7)–C(6)	 122.98(13)
C(11)–O(2)–C(7)–C(10)	116.11(15)	C(11)–O(2)–C(7)–C(8)	 3.61(15)
C(5)–C(6)–C(7)–O(2)	61.58(16)	C(5)–C(6)–C(7)–C(10)	 179.19(14)
C(5)–C(6)–C(7)–C(8)	 51.91(18)	C(11)–O(1)–C(8)–C(9)	114.29(14)
C(11)–O(1)–C(8)–C(7)	 9.10(15)	O(2)–C(7)–C(8)–O(1)	7.55(15)
C(6)–C(7)–C(8)–O(1)	123.40(13)	C(10)–C(7)–C(8)–O(1)	 109.77(14)
O(2)–C(7)–C(8)–C(9)	 114.11(14)	C(6)–C(7)–C(8)–C(9)	1.74(19)
C(10)–C(7)–C(8)–C(9)	128.58(15)	C(5)–C(4)–C(9)–C(8)	 51.0(2)
C(3)–C(4)–C(9)–C(8)	 119.54(18)	O(1)–C(8)–C(9)–C(4)	 69.51(17)
C(7)–C(8)–C(9)–C(4)	49.27(19)	C(7)–O(2)–C(11)–O(1)	 1.77(15)
C(7)–O(2)–C(11)–C(12)	119.06(13)	C(7)–O(2)–C(11)–C(28)	 117.62(12)
C(8)–O(1)–C(11)–O(2)	7.04(15)	C(8)–O(1)–C(11)–C(12)	 114.74(13)
C(8)–O(1)–C(11)–C(28)	123.12(11)	O(2)–C(11)–C(12)–C(17)	 155.60(14)
O(1)–C(11)–C(12)–C(17)	 36.09(18)	C(28)–C(11)–C(12)–C(17)	83.41(17)
O(2)–C(11)–C(12)–C(13)	23.12(19)	O(1)–C(11)–C(12)–C(13)	142.63(14)
C(28)–C(11)–C(12)–C(13)	 97.88(16)	C(17)–C(12)–C(13)–C(14)	1.1(3)
C(11)–C(12)–C(13)–C(14)	 177.66(15)	C(12)–C(13)–C(14)–C(15)	 1.3(3)
C(13)–C(14)–C(15)–C(16)	0.8(3)	C(14)–C(15)–C(16)–C(17)	0.0(4)
C(13)–C(12)–C(17)–C(16)	 0.3(3)	C(11)–C(12)–C(17)–C(16)	178.47(17)
C(15)–C(16)–C(17)–C(12)	 0.3(3)	C(18)–C(20)–C(21)–C(26)	 9.8(3)
C(19)–C(20)–C(21)–C(26)	 153.96(16)	C(22)–C(20)–C(21)–C(26)	100.13(17)
C(18)–C(20)–C(21)–C(22)	 109.9(2)	C(19)–C(20)–C(21)–C(22)	105.92(17)
C(18)–C(20)–C(22)–C(23)	10.6(3)	C(19)–C(20)–C(22)–C(23)	152.55(18)
C(21)–C(20)–C(22)–C(23)	 101.60(17)	C(18)–C(20)–C(22)–C(21)	112.2(2)
C(19)–C(20)–C(22)–C(21)	 105.86(19)	C(26)–C(21)–C(22)–C(23)	 3.86(19)
C(20)–C(21)–C(22)–C(23)	114.42(17)	C(26)–C(21)–C(22)–C(20)	 118.27(17)
C(20)–C(22)–C(23)–C(24)	117.77(17)	C(21)–C(22)–C(23)–C(24)	49.10(19)
C(28)–O(4)–C(24)–C(27)	129.73(16)	C(28)–O(4)–C(24)–C(23)	 109.85(14)
C(28)–O(4)–C(24)–C(25)	10.34(15)	C(22)–C(23)–C(24)–O(4)	76.10(17)
C(22)–C(23)–C(24)–C(27)	 165.80(16)	C(22)–C(23)–C(24)–C(25)	 38.56(19)
C(28)–O(3)–C(25)–C(26)	136.11(12)	C(28)–O(3)–C(25)–C(24)	14.85(15)
O(4)–C(24)–C(25)–O(3)	 14.99(15)	C(27)–C(24)–C(25)–O(3)	 130.84(15)
C(23)–C(24)–C(25)–O(3)	102.65(15)	O(4)–C(24)–C(25)–C(26)	 132.18(14)
C(27)–C(24)–C(25)–C(26)	111.96(17)	C(23)–C(24)–C(25)–C(26)	 14.54(19)
C(20)–C(21)–C(26)–C(25)	 118.20(16)	C(22)–C(21)–C(26)–C(25)	 48.66(19)
O(3)–C(25)–C(26)–C(21)	 56.96(17)	C(24)–C(25)–C(26)–C(21)	58.67(18)
C(24)–O(4)–C(28)–O(3)	 1.58(15)	C(24)–O(4)–C(28)–C(29)	118.00(13)
C(24)–O(4)–C(28)–C(11)	 118.68(12)	C(25)–O(3)–C(28)–O(4)	 8.83(15)
C(25)–O(3)–C(28)–C(29)	 129.37(12)	C(25)–O(3)–C(28)–C(11)	107.94(12)
O(2)–C(11)–C(28)–O(4)	 179.74(10)	O(1)–C(11)–C(28)–O(4)	64.27(13)
C(12)–C(11)–C(28)–O(4)	 56.67(14)	O(2)–C(11)–C(28)–O(3)	63.59(13)
O(1)–C(11)–C(28)–O(3)	 52.40(13)	C(12)–C(11)–C(28)–O(3)	 173.34(11)
O(2)–C(11)–C(28)–C(29)	 57.29(14)	O(1)–C(11)–C(28)–C(29)	 173.28(11)
C(12)–C(11)–C(28)–C(29)	65.78(15)	O(4)–C(28)–C(29)–C(34)	26.54(18)
O(3)–C(28)–C(29)–C(34)	145.26(13)	C(11)–C(28)–C(29)–C(34)	 94.30(15)
O(4)–C(28)–C(29)–C(30)	 152.62(13)	O(3)–C(28)–C(29)–C(30)	 33.90(18)
C(11)–C(28)–C(29)–C(30)	86.54(16)	C(34)–C(29)–C(30)–C(31)	 0.2(3)
C(28)–C(29)–C(30)–C(31)	179.00(16)	C(29)–C(30)–C(31)–C(32)	 0.3(3)
C(30)–C(31)–C(32)–C(33)	0.6(3)	C(31)–C(32)–C(33)–C(34)	 0.5(3)
C(30)–C(29)–C(34)–C(33)	0.3(2)	C(28)–C(29)–C(34)–C(33)	 178.89(15)
C(32)–C(33)–C(34)–C(29)	0.1(3)